Copper Tripeptide-3 · Ex-Vivo Follicle Data

AHK-Cu

Dosage & Dose Escalation Guide

Evidence-based AHK-Cu dosage guide covering Pyo 2007 ex-vivo follicle concentrations, patent animal topical percentages, commercial conventions, GHK-Cu conflation traps, topical math, and the proposed AHK-CU-SCALP-01 protocol. No living human AHK-Cu dose located.

★★★★★4.4(310 reviews)Not FDA Approved · No Human Trial · Topical First
  • Copper Tripeptide-3
  • Ex-Vivo Follicles
  • ≠ GHK-Cu
  • No Validated Injection
Compare Providers
  • AHK-Cu complex

    Ala-His-Lys copper(II) complex (~415.93 g/mol). One-residue change from GHK-Cu alters evidence base.

  • Direct human evidence

    Ex-vivo scalp follicles only — 10⁻¹²–10⁻⁹ M stimulatory; 10⁻⁸–10⁻⁷ M inhibitory.

  • Route anchor

    Patent mouse topical 0.1%/0.5% w/w. Proposed first human program: topical 0.01–0.10% w/v.

How It Works

AHK-Cu is proposed to influence dermal papilla cell viability and ex-vivo follicle elongation in a concentration-dependent, biphasic manner. Mechanistic apoptosis markers were explored at 10⁻⁹ M but clinical hair regrowth, scalp PK, and validated human dosing are unestablished.

Follicle culture signal

  • 10⁻¹²–10⁻⁹ M stimulated elongation and MTT
  • 10⁻⁸–10⁻⁷ M inhibited elongation
  • Ex-vivo only — not a scalp dose

Topical rationale

  • Patent 0.1%/0.5% w/w mouse topical
  • Proposed human arms: 0.01–0.10% w/v
  • Penetration and tox gates required first

Identity traps

  • ≠ GHK-Cu (Copper Tripeptide-1)
  • ALAVAX used GHK + 5-ALA
  • SC µg–mg schedules unvalidated

Result

Ex-Vivo Follicles: Mechanistic

Human Trial: None

Topical %: Convention

Expected Results Over Time

Updated August 2026

AHK-Cu Dosage: Topical Research, Follicle Evidence, and Protocol

Research note: Direct AHK-Cu evidence is one peer-reviewed ex-vivo human-follicle experiment plus patent animal work. No living human has received a validated AHK-Cu dose in controlled research. AHK-Cu ≠ GHK-Cu. The protocol below is a proposed topical investigator-run study — not a personal injection or microneedling plan.

No established human dose. The direct peer-reviewed exposure was a culture concentration: 10⁻¹²–10⁻⁹ M stimulated follicle elongation and dermal papilla MTT signal; 10⁻⁸ and 10⁻⁷ M inhibited elongation.

A 1996 patent reported 0.1% and 0.5% w/w topical AHK:Cu in mice and local intradermal doses — preclinical, not human dosage. Finished products commonly use ~0.05%–1%; DIY often 1–2 mg/mL. Online SC claims (50 µg–2 mg) have no human AHK-Cu study.

The 2016 ALAVAX trial used GHK + 5-ALA, not AHK-Cu. A defensible first human program is topical and staged (0.01%, 0.05%, 0.10% w/v at 1 mL/day × 24 weeks) after formulation, penetration, and tox gates.

AHK-Cu dosage in 30 seconds

QuestionResearch summary
IdentityAla-His-Lys · Copper Tripeptide-3 · ≈415.93 g/mol (1:1 complex)
GHK-Cu (Copper Tripeptide-1) · ALAVAX GHK trial
Human participants on AHK-CuNone in controlled research located
Stimulatory lab range10⁻¹²–10⁻⁹ M (ex-vivo / in-vitro)
Patent mouse topical0.1% and 0.5% w/w
Common commercial topical~0.05%–1% (unvalidated)
Validated injection doseNone located
Proposed first human study0.01% · 0.05% · 0.10% w/v topical × 24 wk

What is AHK-Cu?

AHK-Cu is L-alanyl-L-histidyl-L-lysine (Ala-His-Lys, AHK) complexed with copper(II). INCI: Copper Tripeptide-3. It is not GHK-Cu (Copper Tripeptide-1) — alanine replaces glycine at the N-terminus.

Commonly catalogued 1:1 complex: C15H24CuN6O4, MW ~415.93 g/mol, copper ~15.28% of complex mass. Stoichiometry, counterion, hydration, and assay basis differ by supplier — a label milligram is incomplete without five qualifiers.

Identity gate

Confirm Ala-His-Lys · Copper Tripeptide-3 — not GHK-Cu, ALAVAX, or blends

Matches AHK-Cu identity on this page

L-alanyl-L-histidyl-L-lysine complexed with copper(II). Confirm sequence (Ala not Gly), peptide:copper ratio, counterion, hydration, and intact-complex assay — not HPLC area alone.

AHK-Cu vs GHK-Cu

FeatureAHK-CuGHK-Cu
SequenceAla-His-LysGly-His-Lys
INCICopper Tripeptide-3Copper Tripeptide-1
Direct AHK hair evidencePyo 2007 + patentDifferent literature
Interchangeable doses?NoNo

Current research and regulatory status

No standardized US prescribing dose or approved AHK-Cu drug regimen. No registered interventional trial of AHK-Cu in living human participants was located on ClinicalTrials.gov searches through August 2026.

AHK-Cu appears in cosmetic and research-chemical commerce. Cosmetic INCI naming does not establish a medicine dose or androgenetic alopecia treatment claim. Patent examples document IP history — not regulatory approval.

Human research exposures

“Studied on human hair follicles” is accurate only with “outside the body.” Pyo et al., 2007 used isolated scalp follicles and dermal papilla cells — not scalp application, PK, or clinical regrowth.

Human evidence status

Ex-vivo follicles only — no living participant AHK-Cu dose located

Standardized US prescribing dose
None
Living human treated with AHK-Cu in controlled research
None located
Best direct evidence
Ex-vivo human follicles + dermal papilla cells (2007)
Stimulatory lab range
10⁻¹²–10⁻⁹ M
Inhibitory lab concentrations
10⁻⁸ M (−14.8%) · 10⁻⁷ M (−81.5% elongation)
Patent mouse topical
0.1% and 0.5% w/w AHK:Cu
Validated human SC / injection dose
None located
Human PK / half-life
Not established by any route

Evidence sources vs AHK-Cu dose validity

SourceExposureValidates AHK-Cu human dose?
Pyo 200710⁻¹³–10⁻⁷ M cultureMechanistic only — not topical/systemic dose
ALAVAX 2016GHK + 5-ALA 50–100 mg/mLNo — wrong peptide
Copper Tripeptide-1 cocktail 2018Six-active intradermal mixNo — not AHK-Cu
Online protocolsVariable topical/SCDocuments convention only

At 10⁻⁹ M, Bcl-2 rose and cleaved caspase-3/PARP fell under reported conditions — but apoptotic fraction change was not statistically significant. The paper did not measure VEGF or TGF-β1 for AHK-Cu directly.

Laboratory concentration-response

The Pyo study tested seven orders of magnitude to reveal a biphasic curve — not monotonic “more is better.” Using 415.93 g/mol, stimulatory 10⁻¹²–10⁻⁹ M0.000416–0.416 ng/mL.

Culture concentration

Pyo 2007 molarity → mass concentration (415.93 g/mol)

Upper stimulatory · mechanistic assays

Stimulatory range (Pyo 2007)

ng/mL

4.16e-7

pg/mL

4.16e-4

Molarity

10⁻⁹ M

Culture molarity does not translate to topical % without measured scalp penetration. A 0.1% product is millions of times more concentrated in the bottle than 10⁻⁹ M.

Reported research dosage landscape

Patent 0.1%/0.5% topical, cosmetic ~0.05%–1%, DIY 1–2 mg/mL, and SC 50 µg–2 mg are not one therapeutic range. Injectable claims disagree by 10× or more.

Evidence split

Direct AHK-Cu research vs commercial / online conventions

Direct AHK-Cu research

Ex-vivo / in-vitro + patent animals

Human follicles
10⁻¹²–10⁻⁹ M stimulatory; 10⁻⁸–10⁻⁷ M inhibitory
Patent mouse topical
0.1% and 0.5% w/w · BID Mon–Fri
Patent local ID
0.75–1.50 mg/mouse · rat pups 0.05–0.50 mg
Living human trial
None for AHK-Cu itself
Route with best rationale
Topical scalp (proposed first human program)

Current anecdotal / commercial

Conventions · no human AHK-Cu validation

Finished topicals
~0.05%–1% · once/twice daily
DIY serums
1–2 mg/mL (0.1%–0.2% w/v)
SC injection claims
50 µg–2 mg · daily to 3–5× weekly
Mis-citations
ALAVAX GHK · Copper Tripeptide-1 cocktails
Microneedling stacks
No AHK-Cu monotherapy trial

Topical concentration and application math

mg/mL = 10 × % w/v. Applied mass = concentration × volume. A 0.1% label without pump volume and treated area does not specify daily dose.

Topical math

Concentration × volume → applied complex mass and nominal copper

Concentration (% w/v)

Application volume (mL)

mg/mL

1.00 mg/mL

Applied complex mass

1.000 mg

Nominal copper (1:1 complex)

152.8 µg Cu

Bottle molarity (approx.)

2.4 µM

Formula: mg/mL = 10 × % w/v. Applied mass = mg/mL × volume. Percent label alone does not specify daily dose without treated area and number of applications.

Common concentrations (1 mL application)

% w/vmg/mLApplied mass (1 mL)Nominal Cu (1:1 complex)
0.01%0.1 mg/mL0.1 mg~15.3 µg
0.05%0.5 mg/mL0.5 mg~76.4 µg
0.10%1 mg/mL1 mg~152.8 µg
0.50%5 mg/mL5 mg~764 µg
1.00%10 mg/mL10 mg~1.53 mg

A 0.1% solution is ~2.4 million× the upper stimulatory culture molarity before skin contact — that ratio does not predict follicular overdose; it shows topical % cannot be justified by direct culture matching.

Complete evidence-anchored research protocol (AHK-CU-SCALP-01)

First human program should be topical — follicular target, ex-vivo evidence, patent topical animal data. SC/injection exposes whole body without proof useful intact complex reaches scalp dermal papilla.

Proposed arms: vehicle, 0.01%, 0.05%, 0.10% w/v AHK-Cu · 1 mL once daily to ~100 cm² × 24 weeks (Part B). 0.50% omitted initially despite patent arm because human safety/penetration absent and lab inhibition at higher concentrations.

Proposed protocol

AHK-CU-SCALP-01 — staged topical dose-ranging (investigator-run)

PhaseDurationExposurePurpose
Preclinical gatesBefore enrollmentNoneIdentity, formulation, Franz penetration, dermal tox, exposure margin, bioanalytical validation
Part A lead-in14 days0.01% · 0.05% · 0.10% w/v or vehicle · 1 mL daily24 participants · sentinel dosing · safety/exposure characterization
Part B dose-ranging24 weeksFixed assigned concentration · 1 mL daily to ~100 cm²120 participants · primary NV hair count at week 24
Off-treatment follow-upWeek 28NoneDurability photography and safety after final application

Requires identity, Franz penetration, dermal tox, exposure margin, and validated bioanalysis before enrollment. Microneedling, tattooing, and injection are excluded from the proposed design.

Requires preclinical gates: identity, Franz penetration, dermal tox, exposure margin, validated bioanalysis. Microneedling, tattooing, and injection prohibited in the proposed design.

Patent animal and cell research

US5538945: C3H mice 0.1% and 0.5% w/w topical AHK:Cu (1.1:1) in propylene glycol/ethanol/nonoxynol-9 vehicle · ~0.1 mL BID Mon–Fri. Local ID 0.75–1.50 mg/mouse. Rat pups 0.05–0.50 mg ID after cytarabine.

Patent vehicle and synchronized mouse hair cycle ≠ modern water-based cosmetic serum. No HED presented for local topical/ID exposures.

Why these concentrations were used

Pyo used a wide molar series for dose-response characterization. Patent compared 0.1% vs 0.5% in penetration-enhancing vehicle. Daily/twice-daily cadence and 8–24 week online durations reflect convenience and hair-cycle measurement logistics — not AHK-Cu PK.

Community SC schedules have no demonstrated half-life, bioavailability, or dose-response rationale.

Potential benefits: what has and has not been shown

Claim vs evidence

ClaimCurrent conclusion
Stimulatory signal in human follicle cultureYes — biphasic curve
Clinical hair regrowth in peopleUnproven
Validated topical optimum %Unknown
Validated injectable doseNone
Skin/collagen benefits from GHK literatureIndirect only for AHK-Cu

AHK-Cu safety and side effects

No formal treated-human AHK-Cu safety dataset. Lab data show loss of stimulatory effect at 10⁻⁸–10⁻⁷ M. Plausible topical risks: dermatitis, irritation, staining, sensitization. Systemic copper risk depends on unknown absorption — Wilson disease is a special concern.

Safety monitoring

Biphasic lab signal · topical copper unknowns · no injectable safety program

Laboratory signal
10⁻⁸ and 10⁻⁷ M inhibited ex-vivo follicle elongation — higher concentration reversed effect
Topical risks (plausible)
Erythema, pruritus, contact dermatitis, folliculitis, staining; no formal AHK-Cu AE rates
Systemic copper
Absorption unknown on intact scalp; Wilson disease and liver disease are special concerns
Injection unknowns
No human AHK-Cu injectable safety program; research vial ≠ sterile/endotoxin-controlled product

Product quality and storage

Require sequence, stereochemistry, peptide:copper ratio, intact-complex vs free peptide/copper, related impurities, microbial limits (topical), sterility/endotoxin (injectable). 99% HPLC purity does not confirm complexation, correct sequence (vs GHK), or preservative stability.

Storage is product-specific. Blue color suggests copper complexation but does not replace analytical release testing.

Common claims vs evidence

Claim checker

Common AHK-Cu claims vs the evidence record

There is a standard AHK-Cu human dose

False

No living participant has received a controlled AHK-Cu treatment dose. Product percentages are formulation conventions.

AHK-Cu dosage evidence ladder

Dosage evidence ladder

Ex-vivo signal exists — clinical scalp dose does not

LevelWhat existsConfidence
Approved medicinal dosingNoneNone
Human clinical-trial dosingNone for AHK-Cu in living participantsNone
Ex-vivo / in-vitro human tissuePyo 2007 · 10⁻¹³–10⁻⁷ MMechanistic · not a scalp dose
Patent animal dosing0.1%/0.5% topical · local ID in mice/ratsPreclinical · not peer-reviewed trials
Anecdotal topical~0.05%–1% · 8–24 weeksVery low
Anecdotal injection~0.05–2 mg SC · conflicting schedulesInsufficient

AHK-Cu dosing is not clinically established. The next step is a staged topical dose-ranging trial with measured follicular exposure — not selecting an online “standard dose.”

Sports and anti-doping considerations

AHK-Cu is not named on the 2026 WADA list reviewed — not automatic clearance. S0 may apply. Tested athletes need written product-specific guidance; contamination and undisclosed ingredients add risk.

Bottom line

AHK-Cu has one useful human-tissue concentration-response study and patent animal topical/intradermal examples. No living human AHK-Cu dose exists. Topical 0.05%–1% and SC µg–mg schedules are extrapolations; GHK-Cu and ALAVAX citations do not validate AHK-Cu.

Concentration selection matters — higher lab concentrations inhibited follicle elongation. Proposed first human program: 0.01% / 0.05% / 0.10% w/v topical after full CMC and penetration gates.

Ex-vivo human follicles ≠ clinical scalp dose. AHK-Cu ≠ GHK-Cu. Higher % or SC mg without human data is convention, not evidence.

Frequently asked questions

What is the standard AHK-Cu dose?

There is no standard human dose. Finished topicals often use roughly 0.05%–1%, but that reflects products and convention rather than controlled optimization.

Has AHK-Cu been tested in a human clinical trial?

No controlled study administering AHK-Cu to living participants was located. Human follicles were studied ex-vivo in 2007.

What concentration was active in the Pyo study?

AHK-Cu stimulated follicle elongation and dermal papilla MTT signal from 10⁻¹² to 10⁻⁹ M. Ten⁻⁸ and 10⁻⁷ M inhibited elongation.

Is AHK-Cu the same as GHK-Cu?

No. AHK-Cu is Ala-His-Lys (Copper Tripeptide-3). GHK-Cu is Gly-His-Lys (Copper Tripeptide-1). Doses are not interchangeable.

Did the ALAVAX study test AHK-Cu?

No. It tested 5-aminolevulinic acid plus GHK peptide at 50 or 100 mg/mL once daily for six months.

What topical percentages were used in animals?

A patent mouse experiment used 0.1% and 0.5% w/w AHK:Cu in a penetration-enhancing vehicle, applied about 0.1 mL twice daily Monday–Friday.

What is the injectable AHK-Cu dose?

None is established. Online claims range from tens of micrograms to 2 mg with conflicting schedules — no published human injection study.

Can I match topical % to the culture molarity?

No. A 0.1% product is millions of times more concentrated in the bottle than the stimulatory culture range; skin penetration is unknown and inefficient.

Does AHK-Cu regrow hair in people?

Unproven. The ex-vivo signal supports a controlled trial, but no randomized human AHK-Cu regrowth study was located.

Can a 50 mg vial be reconstituted for injection?

Adding liquid yields a concentration, not injectable suitability. Research material may lack sterility, endotoxin control, and a supported human dose.

References

Latest Research on AHK-Cu

Stay updated on the latest peptide research

New studies and guides delivered to your inbox.